ARTICLE
TITLE

Quality evaluation of the measurement of total carbon in soil by an inter-comparison assay.

SUMMARY

The Mexican regulation NMX-EC-17025-IMNC-2006, establishes that laboratories must have quality control procedures to monitor the validity of tests and calibrations, such monitoring must be planned and reviewed with: a) the regular use of certif?ied reference materials or internal quality control of secondary references; b) participation in inter-laboratory comparisons or a prof?iciency testing program; c) the repetition of tests or calibrations using the same method or different methods; d) the repetition of the test or the calibration of determined objects; e) the correlation of results for different characteristics of a reference material certif?ied by MRC. The quality evaluation of results from the eight laboratories of the Laboratory Network for Analysis, Use, Conservation and Management of Soil (REDLABS) included the elements of sections a), b), c), and d) in order to verify the hypothesis that laboratories emit repeatable, reproducible and unbiased results. In our study, elemental analyzers of different brands were used to measure the total carbon of soil. A certif?ied reference material was included in the Inter-comparison Practice. Repeatability and reproducibility of the carbon analyzes were evaluated with samples from the inter-comparison practice; the precision of analyzes from each laboratory was qualif?ied with MRC. The results obtained indicate that the laboratories show repeatability in their analyzes with no statistical differences, i.e. reproducibility is detected by inter-comparison. The data issued by the laboratories were unbiased according to their evaluation with certif?ied reference material.

 Articles related

Fikret Ustaoglu    

Dams are important sources particularly for energy production as well as drinking and irrigation water. In this study, dissolved metal concentrations in Degirmendere Dam water in Amasya province were determined by ICP-MS and the data were evaluated in te... see more


Seda TUNÇAY ÇAGATAY,Gülsah ÇALIK KOÇ,Fereshteh REZAEI,Özlem DARCANSOY ISERI,Feride Iffet SAHIN,Mehmet HABERAL    

This study aimed to investigate the effects of grafting tomato on different tobacco rootstocks on quality factors and nicotine content. The commercial variety (Solanum lycopersicum ‘H2274’) (BIOTECH) of the tomato was used as the scion plant, and six dif... see more


Fernando Magdaleno,Roberto Martínez    

Aim of study: This paper presents a novel index, the Riparian Forest Evaluation (RFV) index, for assessing the ecological condition of riparian forests. The status of riparian ecosystems has global importance due to the ecological and social benefits and... see more

Revista: Forest Systems

Franco Famiani,Daniela Farinelli,Sara Rollo,Salvatore Camposeo,Claudio Di Vaio,Paolo Inglese    

In 2006 and 2009, trials were carried out in the Apulia region in Southern Italy to evalu-ate the possibility of mechanizing olive harvesting in groves of old and very large trees. The trees belonged to the cultivars ‘Cellina di Nardò’ and ‘Ogliarola Sal... see more


Azize Dogan Demir,Yasin Demir    

Most of the non-irrigated areas in the southeast of the Harran Plain are irrigated by groundwater. The aim of this study is to determine the importance of 13 underground irrigation water sources operating in the agricultural areas of Ohali village in sou... see more